Paladium and Silver recovery & refining from MLCC part 1

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Kind: captions
Language: en

00:00:00.430
[Music]
00:00:39.230 00:00:39.240 hey guys what's up so today we've got
00:00:44.550 00:00:44.560 some new stuff for you
00:00:47.630 00:00:47.640 okay this is the ML TT monoatomic
00:00:52.580 00:00:52.590 capacitor so what we do today is the we
00:00:58.799 00:00:58.809 try to recover some silver and palladium
00:01:02.420 00:01:02.430 maybe some gold from that
00:01:05.420 00:01:05.430 immensities here I got about two hundred
00:01:12.060 00:01:12.070 and eighty grand grams death penalty T's
00:01:17.060 00:01:17.070 280 grams almost 300 grams so if you see
00:01:22.889 00:01:22.899 inside we got a lot of species we've got
00:01:27.120 00:01:27.130 some big one and the small one see that
00:01:33.990 00:01:34.000 big one that big one got some this one
00:01:38.100 00:01:38.110 this is not the NLCC sometimes it is
00:01:40.859 00:01:40.869 sometimes not but it's got couple inside
00:01:45.660 00:01:45.670 your mind
00:01:46.680 00:01:46.690 got some fishes precious metal - maybe
00:01:49.499 00:01:49.509 some silver very at 110 - so what I do
00:01:55.740 00:01:55.750 for the first is I want to cross that
00:01:59.490 00:01:59.500 stuff to the finest in final dust and I
00:02:04.320 00:02:04.330 do that hammer same little chips so
00:02:08.580 00:02:08.590 maybe for some of you this is not a good
00:02:11.250 00:02:11.260 way but for the small amount that I have
00:02:14.370 00:02:14.380 now see that okay for crushing I use my
00:02:25.199 00:02:25.209 show you proportionality I use this
00:02:28.650 00:02:28.660 system this is the Train part of the
00:02:33.089 00:02:33.099 Train rode for train so just various
00:02:40.949 00:02:40.959 buckets because I don't splash about the
00:02:44.309 00:02:44.319 other side
00:02:47.589 00:02:47.599 or just this this way QRF both side
00:03:10.270 00:03:10.280 percent son bottom spread cast or if you
00:03:54.909 00:03:54.919 eat that easier for you you can do it
00:03:57.789 00:03:57.799 like this just put that in some metal
00:04:01.210 00:04:01.220 can't this is my stainless steel pot and
00:04:10.920 00:04:10.930 kicking okay I think I grind out enough
00:04:15.580 00:04:15.590 pretty cool still got some bigger pieces
00:04:19.680 00:04:19.690 see that but never mind
00:04:22.290 00:04:22.300 so often do next I got this big job
00:04:27.700 00:04:27.710 because the bigger surface surface
00:04:29.770 00:04:29.780 surface for acid attack and I use my
00:04:35.100 00:04:35.110 that dish just because this jar got
00:04:40.659 00:04:40.669 crack see that bigger crack but I think
00:04:47.110 00:04:47.120 it's hole in the side so what did you
00:04:51.820 00:04:51.830 have to do now we got some
00:04:55.900 00:04:55.910 anaphoric acid I put that inside to eat
00:04:59.920 00:04:59.930 all the base metal beyond that reaction
00:05:20.400 00:05:20.410 now that too much because when the pod
00:05:25.300 00:05:25.310 stop we will be can this and repeat that
00:05:28.810 00:05:28.820 process for for two days so what we do
00:05:33.010 00:05:33.020 next itself believe this for couple days
00:05:38.200 00:05:38.210 the hello Coral Castle eat all that
00:05:43.380 00:05:43.390 nickel because we don't want to call in
00:05:46.750 00:05:46.760 a final product silver and palladium
00:05:54.210 00:05:54.220 just what you need to do is the royal
00:05:58.180 00:05:58.190 couple all right let me show that I got
00:06:02.860 00:06:02.870 that week because that dust just sitting
00:06:10.270 00:06:10.280 in a bottle
00:06:32.330 00:06:32.340 it's pretty hot reaction
00:06:39.630 00:06:39.640 00:06:42.980 00:06:42.990 read-modify-write okay it's passed over
00:06:51.210 00:06:51.220 two days and the ID tent in the first
00:06:56.490 00:06:56.500 HCl social so okay of the left
00:07:03.530 00:07:03.540 it's a bite slug and you see that ml
00:07:10.950 00:07:10.960 city's this white stuff it's a silver
00:07:17.220 00:07:17.230 chloride so I filter that HCL solution
00:07:22.280 00:07:22.290 because I wanna keep all that sugar for
00:07:25.740 00:07:25.750 right in the hip when the filter will
00:07:29.730 00:07:29.740 charm Punk not Bonnie's filters and see
00:07:34.350 00:07:34.360 that the black and the black color
00:07:37.560 00:07:37.570 resolution this is the indicate it's a
00:07:40.020 00:07:40.030 nickel in the solution so what I do next
00:07:45.900 00:07:45.910 is I add more HCL just to be sure that I
00:07:52.070 00:07:52.080 leave it for more two days just before
00:07:54.930 00:07:54.940 that I dissolve all the nickel
00:08:03.210 00:08:03.220 this is just how it's white this is all
00:08:07.380 00:08:07.390 the silver everything right in the
00:08:10.170 00:08:10.180 silver okay
00:08:19.540 00:08:19.550 okay after for five days we remove with
00:08:25.839 00:08:25.849 a HCl hydrochloric acid that we remove
00:08:28.990 00:08:29.000 all that nickel and somebody probably
00:08:33.459 00:08:33.469 say why not straight go to nitric acid
00:08:39.250 00:08:39.260 and dissolve and the nickel and the
00:08:41.170 00:08:41.180 silver and later remove drop some silver
00:08:46.449 00:08:46.459 from the nitric acid but we can do that
00:08:49.810 00:08:49.820 because we got much much solder lead and
00:08:53.440 00:08:53.450 in tin and lead inside
00:08:56.440 00:08:56.450 so the first step it's always HCL to
00:09:00.220 00:09:00.230 remove tin lead and that's older and
00:09:04.350 00:09:04.360 that nickel so now we D can't all that
00:09:10.019 00:09:10.029 second solution and the bottom we don't
00:09:14.500 00:09:14.510 got any superfluid stay on filter but
00:09:19.810 00:09:19.820 now we need the wash rinse that stuff
00:09:25.110 00:09:25.120 that analogy several time with a water
00:09:28.780 00:09:28.790 to remove all that left HCL because the
00:09:34.269 00:09:34.279 next step is a nitric batch that inside
00:09:38.010 00:09:38.020 the resolve to dissolve that silver and
00:09:42.180 00:09:42.190 leave I hope palladium so what we need
00:09:46.990 00:09:47.000 this now what we need to do it's a dwarf
00:09:50.380 00:09:50.390 that slug several times and remove all
00:09:55.000 00:09:55.010 that itself okay
00:09:58.060 00:09:58.070 I was that several times but we still
00:10:01.870 00:10:01.880 got some circle right inside I think I
00:10:04.870 00:10:04.880 remove every HCl that maybe stays on
00:10:11.590 00:10:11.600 inside not make such a big problem that
00:10:17.400 00:10:17.410 zero zero one percent and what I want to
00:10:21.069 00:10:21.079 show you now to see that from the top
00:10:25.750 00:10:25.760 this is all the palladium foils
00:10:29.670 00:10:29.680 okay
00:10:31.200 00:10:31.210 now I will add nitric acid in that to
00:10:35.770 00:10:35.780 dissolve all that silver and when this
00:10:40.150 00:10:40.160 is finished filtering neither too much
00:10:43.990 00:10:44.000 time I will put that several fluoride in
00:10:47.890 00:10:47.900 this after I rinse came from the HCL and
00:10:54.510 00:10:54.520 okay now now I will make mix calf nitric
00:11:11.860 00:11:11.870 set water
00:11:19.860 00:11:33.639 00:11:33.649 this is not supposed to happen probably
00:11:49.880 00:11:49.890 say some other colic acid inside I wash
00:11:55.610 00:11:55.620 several times but maybe space am okay
00:12:00.319 00:12:00.329 now my so we'll leave it to dissolve and
00:12:07.240 00:12:07.250 main job is finished
00:12:10.810 00:12:10.820 00:12:26.130 00:12:26.140 hey guys so this is our silver for life
00:12:32.250 00:12:32.260 and I dropped that so I D can that
00:12:39.130 00:12:39.140 solution from this MLT T's this is the
00:12:42.190 00:12:42.200 filter inside and what I do love them
00:12:46.120 00:12:46.130 the next is I add HCl to drop that
00:12:50.710 00:12:50.720 silver and if you see that unbuttoned
00:12:53.020 00:12:53.030 already gasps you all right
00:12:54.760 00:12:54.770 now you have that the settles down but
00:12:57.730 00:12:57.740 you see that color is not white he's got
00:13:01.630 00:13:01.640 something some yellow so I think I got
00:13:07.180 00:13:07.190 some HCL still that entities and I
00:13:12.060 00:13:12.070 dissolve some palladium inside but never
00:13:17.740 00:13:17.750 mind when I filtered that silver I drop
00:13:25.090 00:13:25.100 that plating from that person okay and
00:13:30.430 00:13:30.440 now we will add some aqua video here
00:13:34.510 00:13:34.520 dissolve a analyst relating to steak
00:13:38.430 00:13:38.440 that's ironic
00:14:12.740 00:14:12.750 okay this is our Spanish test and she
00:14:16.680 00:14:16.690 got palsy we got a positive for
00:14:19.320 00:14:19.330 palladium this is from this one and this
00:14:28.050 00:14:28.060 is our second but
00:15:06.260 00:15:06.270
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