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Paladium and Silver recovery & refining from MLCC part 1
WEBVTT Kind: captions Language: en
00:00:00.430 [Music] 00:00:39.23000:00:39.240 hey guys what's up so today we've got 00:00:44.55000:00:44.560 some new stuff for you 00:00:47.63000:00:47.640 okay this is the ML TT monoatomic 00:00:52.58000:00:52.590 capacitor so what we do today is the we 00:00:58.79900:00:58.809 try to recover some silver and palladium 00:01:02.42000:01:02.430 maybe some gold from that 00:01:05.42000:01:05.430 immensities here I got about two hundred 00:01:12.06000:01:12.070 and eighty grand grams death penalty T's 00:01:17.06000:01:17.070 280 grams almost 300 grams so if you see 00:01:22.88900:01:22.899 inside we got a lot of species we've got 00:01:27.12000:01:27.130 some big one and the small one see that 00:01:33.99000:01:34.000 big one that big one got some this one 00:01:38.10000:01:38.110 this is not the NLCC sometimes it is 00:01:40.85900:01:40.869 sometimes not but it's got couple inside 00:01:45.66000:01:45.670 your mind 00:01:46.68000:01:46.690 got some fishes precious metal - maybe 00:01:49.49900:01:49.509 some silver very at 110 - so what I do 00:01:55.74000:01:55.750 for the first is I want to cross that 00:01:59.49000:01:59.500 stuff to the finest in final dust and I 00:02:04.32000:02:04.330 do that hammer same little chips so 00:02:08.58000:02:08.590 maybe for some of you this is not a good 00:02:11.25000:02:11.260 way but for the small amount that I have 00:02:14.37000:02:14.380 now see that okay for crushing I use my 00:02:25.19900:02:25.209 show you proportionality I use this 00:02:28.65000:02:28.660 system this is the Train part of the 00:02:33.08900:02:33.099 Train rode for train so just various 00:02:40.94900:02:40.959 buckets because I don't splash about the 00:02:44.30900:02:44.319 other side 00:02:47.58900:02:47.599 or just this this way QRF both side 00:03:10.27000:03:10.280 percent son bottom spread cast or if you 00:03:54.90900:03:54.919 eat that easier for you you can do it 00:03:57.78900:03:57.799 like this just put that in some metal 00:04:01.21000:04:01.220 can't this is my stainless steel pot and 00:04:10.92000:04:10.930 kicking okay I think I grind out enough 00:04:15.58000:04:15.590 pretty cool still got some bigger pieces 00:04:19.68000:04:19.690 see that but never mind 00:04:22.29000:04:22.300 so often do next I got this big job 00:04:27.70000:04:27.710 because the bigger surface surface 00:04:29.77000:04:29.780 surface for acid attack and I use my 00:04:35.10000:04:35.110 that dish just because this jar got 00:04:40.65900:04:40.669 crack see that bigger crack but I think 00:04:47.11000:04:47.120 it's hole in the side so what did you 00:04:51.82000:04:51.830 have to do now we got some 00:04:55.90000:04:55.910 anaphoric acid I put that inside to eat 00:04:59.92000:04:59.930 all the base metal beyond that reaction 00:05:20.40000:05:20.410 now that too much because when the pod 00:05:25.30000:05:25.310 stop we will be can this and repeat that 00:05:28.81000:05:28.820 process for for two days so what we do 00:05:33.01000:05:33.020 next itself believe this for couple days 00:05:38.20000:05:38.210 the hello Coral Castle eat all that 00:05:43.38000:05:43.390 nickel because we don't want to call in 00:05:46.75000:05:46.760 a final product silver and palladium 00:05:54.21000:05:54.220 just what you need to do is the royal 00:05:58.18000:05:58.190 couple all right let me show that I got 00:06:02.86000:06:02.870 that week because that dust just sitting 00:06:10.27000:06:10.280 in a bottle 00:06:32.33000:06:32.340 it's pretty hot reaction 00:06:39.63000:06:39.64000:06:42.98000:06:42.990 read-modify-write okay it's passed over 00:06:51.21000:06:51.220 two days and the ID tent in the first 00:06:56.49000:06:56.500 HCl social so okay of the left 00:07:03.53000:07:03.540 it's a bite slug and you see that ml 00:07:10.95000:07:10.960 city's this white stuff it's a silver 00:07:17.22000:07:17.230 chloride so I filter that HCL solution 00:07:22.28000:07:22.290 because I wanna keep all that sugar for 00:07:25.74000:07:25.750 right in the hip when the filter will 00:07:29.73000:07:29.740 charm Punk not Bonnie's filters and see 00:07:34.35000:07:34.360 that the black and the black color 00:07:37.56000:07:37.570 resolution this is the indicate it's a 00:07:40.02000:07:40.030 nickel in the solution so what I do next 00:07:45.90000:07:45.910 is I add more HCL just to be sure that I 00:07:52.07000:07:52.080 leave it for more two days just before 00:07:54.93000:07:54.940 that I dissolve all the nickel 00:08:03.21000:08:03.220 this is just how it's white this is all 00:08:07.38000:08:07.390 the silver everything right in the 00:08:10.17000:08:10.180 silver okay 00:08:19.54000:08:19.550 okay after for five days we remove with 00:08:25.83900:08:25.849 a HCl hydrochloric acid that we remove 00:08:28.99000:08:29.000 all that nickel and somebody probably 00:08:33.45900:08:33.469 say why not straight go to nitric acid 00:08:39.25000:08:39.260 and dissolve and the nickel and the 00:08:41.17000:08:41.180 silver and later remove drop some silver 00:08:46.44900:08:46.459 from the nitric acid but we can do that 00:08:49.81000:08:49.820 because we got much much solder lead and 00:08:53.44000:08:53.450 in tin and lead inside 00:08:56.44000:08:56.450 so the first step it's always HCL to 00:09:00.22000:09:00.230 remove tin lead and that's older and 00:09:04.35000:09:04.360 that nickel so now we D can't all that 00:09:10.01900:09:10.029 second solution and the bottom we don't 00:09:14.50000:09:14.510 got any superfluid stay on filter but 00:09:19.81000:09:19.820 now we need the wash rinse that stuff 00:09:25.11000:09:25.120 that analogy several time with a water 00:09:28.78000:09:28.790 to remove all that left HCL because the 00:09:34.26900:09:34.279 next step is a nitric batch that inside 00:09:38.01000:09:38.020 the resolve to dissolve that silver and 00:09:42.18000:09:42.190 leave I hope palladium so what we need 00:09:46.99000:09:47.000 this now what we need to do it's a dwarf 00:09:50.38000:09:50.390 that slug several times and remove all 00:09:55.00000:09:55.010 that itself okay 00:09:58.06000:09:58.070 I was that several times but we still 00:10:01.87000:10:01.880 got some circle right inside I think I 00:10:04.87000:10:04.880 remove every HCl that maybe stays on 00:10:11.59000:10:11.600 inside not make such a big problem that 00:10:17.40000:10:17.410 zero zero one percent and what I want to 00:10:21.06900:10:21.079 show you now to see that from the top 00:10:25.75000:10:25.760 this is all the palladium foils 00:10:29.67000:10:29.680 okay 00:10:31.20000:10:31.210 now I will add nitric acid in that to 00:10:35.77000:10:35.780 dissolve all that silver and when this 00:10:40.15000:10:40.160 is finished filtering neither too much 00:10:43.99000:10:44.000 time I will put that several fluoride in 00:10:47.89000:10:47.900 this after I rinse came from the HCL and 00:10:54.51000:10:54.520 okay now now I will make mix calf nitric 00:11:11.86000:11:11.870 set water 00:11:19.86000:11:33.63900:11:33.649 this is not supposed to happen probably 00:11:49.88000:11:49.890 say some other colic acid inside I wash 00:11:55.61000:11:55.620 several times but maybe space am okay 00:12:00.31900:12:00.329 now my so we'll leave it to dissolve and 00:12:07.24000:12:07.250 main job is finished 00:12:10.81000:12:10.82000:12:26.13000:12:26.140 hey guys so this is our silver for life 00:12:32.25000:12:32.260 and I dropped that so I D can that 00:12:39.13000:12:39.140 solution from this MLT T's this is the 00:12:42.19000:12:42.200 filter inside and what I do love them 00:12:46.12000:12:46.130 the next is I add HCl to drop that 00:12:50.71000:12:50.720 silver and if you see that unbuttoned 00:12:53.02000:12:53.030 already gasps you all right 00:12:54.76000:12:54.770 now you have that the settles down but 00:12:57.73000:12:57.740 you see that color is not white he's got 00:13:01.63000:13:01.640 something some yellow so I think I got 00:13:07.18000:13:07.190 some HCL still that entities and I 00:13:12.06000:13:12.070 dissolve some palladium inside but never 00:13:17.74000:13:17.750 mind when I filtered that silver I drop 00:13:25.09000:13:25.100 that plating from that person okay and 00:13:30.43000:13:30.440 now we will add some aqua video here 00:13:34.51000:13:34.520 dissolve a analyst relating to steak 00:13:38.43000:13:38.440 that's ironic 00:14:12.74000:14:12.750 okay this is our Spanish test and she 00:14:16.68000:14:16.690 got palsy we got a positive for 00:14:19.32000:14:19.330 palladium this is from this one and this 00:14:28.05000:14:28.060 is our second but 00:15:06.26000:15:06.270
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