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Paladium and Silver recovery & refining from MLCC part 2
WEBVTT Kind: captions Language: en
00:00:00.430 [Music] 00:00:44.44000:00:44.450 okay guys after a couple of washes with 00:00:47.77000:00:47.780 aquilegia I put some nitric in that 00:00:51.57000:00:51.580 leftover ceramic and you see that just a 00:00:56.11000:00:56.120 little bit silver on the nitric so our 00:01:00.72900:01:00.739 job is finished this is only ceramic so 00:01:05.26000:01:05.270 I already got one batch on vaporize 00:01:09.40000:01:09.410 process and this is my main but I got 00:01:15.13000:01:15.140 this I got a couple of batches and this 00:01:20.92000:01:20.930 is the last one which is a filter so now 00:01:26.17000:01:26.180 I'll just wait little bit to nitric this 00:01:28.96000:01:28.970 is all walnut silver and this is a 00:01:33.60900:01:33.619 training water waste the weight that the 00:01:37.03000:01:37.040 filter and we made that silver filter 00:01:39.82000:01:39.830 see that oh okay and all that job 00:01:46.15000:01:46.160 finished all back guys okay we will 00:01:51.19000:01:51.200 filter all this so you see that this is 00:01:55.35900:01:55.369 all our aqua regia solution because I 00:01:58.80900:01:58.819 got a mistake I never a good wash I 00:02:02.08000:02:02.090 don't have a good wash from HCl on the 00:02:04.77900:02:04.789 first so this is these two are the first 00:02:08.29000:02:08.300 a Kavita and this to our second ecology 00:02:12.67000:02:12.680 so this is the best Olivia 00:02:14.53000:02:14.540 and this is the first one because we had 00:02:19.18000:02:19.190 in that nitric acid we had more 00:02:23.19900:02:23.209 alcoholic acid reduce and make aquilegia 00:02:26.41000:02:26.420 because we nirvash good mlct 00:02:31.63000:02:31.640 from that first batch when we remove 00:02:34.33000:02:34.340 lead and tin but nevermind okay we put 00:02:38.71000:02:38.720 that to vaporize on the Sun we don't use 00:02:42.52000:02:42.530 any heat because still I maybe do show 00:02:47.38000:02:47.390 you how to cheap and easy without any 00:02:51.30900:02:51.319 technology removing recover 00:02:54.79000:02:54.800 vicious metal from the e-waste so this 00:02:58.52000:02:58.530 is we live through our eyes to reduce 00:03:03.37000:03:03.380 amount of liquid and leave that liquid 00:03:08.69000:03:08.700 without a nitric and these however this 00:03:12.22900:03:12.239 is our silver chloride not bad is a 00:03:18.86000:03:18.870 heavy and I leave that to the price may 00:03:23.90000:03:23.910 cry and when this is made right we go 00:03:27.89000:03:27.900 and that convert silver nitrate with the 00:03:33.11000:03:33.120 Y and sugar water and okay when all that 00:03:37.69900:03:37.709 we finish our back to show you but next 00:03:41.63000:03:41.640 step is okay in the meantime this is our 00:03:49.28000:03:49.290 silver chloride that's the awesome water 00:03:52.28000:03:52.290 but my mind should be wet when we do 00:03:56.35000:03:56.360 that stuff with by so what we do next 00:04:00.17000:04:00.180 that we are convert civil right to 00:04:04.43000:04:04.440 silver nitrate with a lie and sugar 00:04:08.39000:04:08.400 water okay so let's start 00:04:25.83000:04:25.840 you see how it's change his color and 00:04:43.20000:04:43.210 it's be very hot is be enough see how 00:05:10.99000:05:11.000 it's going dark okay what we do next we 00:05:25.33000:05:25.340 got sugar water sugar dissolve in that 00:05:29.05000:05:29.060 water and we add this 00:05:46.04000:05:46.050 okay we add just a little bit so what we 00:05:56.85000:05:56.860 do next I will meet that redwood and 00:06:00.11000:06:00.120 I'll back that from the that magical on 00:06:04.74000:06:04.750 the Sun and leave it to vaporize that 00:06:13.23000:06:13.240 extra water and we go to straighten out 00:06:17.31000:06:17.320 okay guys I'm not be satisfied with the 00:06:22.44000:06:22.450 purity of my silver nitrate so I really 00:06:31.05000:06:31.060 fine 00:06:31.59000:06:31.600 look what crap I got I don't know really 00:06:36.18000:06:36.190 what is that thing but I rather find 00:06:41.82000:06:41.830 that and I got my silver chloride see 00:06:48.48000:06:48.490 that and now I filter this see that King 00:06:54.42000:06:54.430 good oh okay 00:06:59.37000:06:59.380 you see that this is this tossed it look 00:07:03.03000:07:03.040 like silver horrid but it's not so 00:07:07.50000:07:07.510 alright this is a variety and this is a 00:07:11.64000:07:11.650 whole ride 00:07:12.42000:07:12.430 this is not support all right this is 00:07:14.91000:07:14.920 what what it's left from so a silver 00:07:22.86000:07:22.870 night night wait when I verifying that 00:07:27.02000:07:27.030 so I really don't know what is this 00:07:30.30000:07:30.310 white stuff but isn't so polite okay 00:07:38.17000:07:38.180 my filter is very good this is nothing 00:08:00.89000:08:00.900 this is my home crucible this is we use 00:08:08.15000:08:08.160 for salt this is some kind of ceramic 00:08:13.90000:08:13.910 can do for gold or for anything else but 00:08:18.62000:08:18.630 for the silver it's very good so okay 00:08:21.02000:08:21.030 this is the bit that beaded nice little 00:08:25.34000:08:25.350 chunk this is the silver from our adult 00:08:30.37900:08:30.389 cities and I note him in this I can't my 00:08:38.99000:08:39.000 wittle port is bad I can melt I can only 00:08:44.72000:08:44.730 collect him and then that little pile I 00:08:49.10000:08:49.110 will take outside in this little break 00:08:54.32000:08:54.330 and here I melt him to the end okay now 00:09:00.76900:09:00.779 we see so we got silver from 207 270 00:09:10.79000:09:10.800 gram mlct 3.6 grand Kosovo okay okay 00:09:22.76000:09:22.770 conceal run cool this is our aqua regia 00:09:31.91000:09:31.920 I will not vaporize I realized that on 00:09:37.31000:09:37.320 Sun for today and I will not add on 00:09:42.35000:09:42.360 extra heat to reduce that to here sighs 00:09:46.09000:09:46.100 now I will add ammonium chloride to 00:09:50.03000:09:50.040 precipitate 00:09:51.23000:09:51.240 some Clayton another idea metal and 00:09:58.96000:09:58.970 prepare palladium for drop with the for 00:10:04.55000:10:04.560 India's and give that to settle 00:10:51.32000:10:51.330 overnight and we will see tomorrow is if 00:10:56.51000:10:56.520 there is there any slug on a button and 00:11:06.47000:11:06.480 we will do the same our first date 00:11:08.78000:11:08.790 remember that - spoon same light cruiser 00:11:24.98000:11:24.990 and I will not dissolve that ammonium 00:11:31.10000:11:31.110 fluoride in the water to make 00:11:32.86000:11:32.870 concentrate solution just right all 00:11:39.07900:11:39.089 right okay and the same we got some 00:11:49.46000:11:49.470 change color here and for the same we 00:11:53.51000:11:53.520 leave that good morning 00:12:13.74000:12:13.750 I'm confused okay we got some slide 00:12:22.13900:12:22.149 right a moment and we start it started 00:12:26.65000:12:26.660 rot it look like some Palladium 00:12:32.40000:12:32.410 because that way we should get some red 00:12:37.54000:12:37.550 brick radium and okay that car pretty 00:12:47.23000:12:47.240 music see I'll catch a jar and our 00:12:57.30900:12:57.319 brother is the same okay I will let that 00:13:09.42900:13:09.439 settle down we will see what we got but 00:13:14.85000:13:14.860 pretty strange for me okay guys it's and 00:13:21.06900:13:21.079 I just can't wait to show you 00:13:24.67000:13:24.680 I will check what is going on with my 00:13:27.29900:13:27.309 aqua Regius ocean and look all this 00:13:31.05900:13:31.069 stuff this is on the top just some walls 00:13:40.60000:13:40.610 but they already settled down and look 00:13:44.86000:13:44.870 this local that palladium we we got just 00:13:51.69900:13:51.709 with ammonium chloride we got our play 00:13:56.23000:13:56.240 diem see that again see that on the 00:13:59.94900:13:59.959 middle we got some salt heavy salt 00:14:04.03000:14:04.040 I think it's plating not sure so 00:14:07.17900:14:07.189 probably our play do not be clean but 00:14:09.28000:14:09.290 look all that size of palladium look at 00:14:19.01900:14:19.029 Petco isn't 00:14:22.37900:14:22.389 okay tomorrow we collect all this and we 00:14:27.80900:14:27.819 melt this but not with my torch I go to 00:14:31.26900:14:31.279 my friend and mean and me that much he 00:14:36.91000:14:36.920 got a much stronger torch and beautiful 00:14:40.44900:14:40.459 probably it would be very fun to see 00:14:42.97000:14:42.980 what we got 00:14:51.23900:14:51.249 hey guys 00:14:53.04000:14:53.050 so after this settle down but not all I 00:15:03.05900:15:03.069 I feel that yet so I felt for that and 00:15:16.61900:15:16.629 I'll leave it this is just a first tour 00:15:21.63900:15:21.649 we got other look that that gets for 00:15:29.46000:15:29.470 little cool 00:15:51.25000:15:51.260 okay I'll back my filter guys we still 00:16:02.90000:16:02.910 filtering it's already night eleven 00:16:08.15000:16:08.160 o'clock you see I got very clean 00:16:14.00000:16:14.010 solution and this is our red brick 00:16:28.47000:16:28.480
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